All crucibles is often simply loaded or faraway from the TGA or DSC measuring cell—either manually or quickly—utilizing the sample robotic. Automated lid removal and piercing in advance of measurment prevents the uptake of humidity and sample contamination.
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The sort of crucible useful for a measurement might have a substantial effect on the caliber of the final results obtained and could also affect vital qualities of the DSC signal.
Alumina crucibles are used for TGA/DSC also, but the heat flow signal (SDTA) are going to be suppressed. It is not suggested to employ such a crucible for DSC measurements. These crucibles may be simply cleaned and reused.
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Along with the diversity of components offered, for example Alumina, Zirconia, or Magnesium Oxide, it really is important to select the right style of crucible for your precise application.
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Most often, the forty μL pan is utilized in combination with a regular lid into which a large gap has been more info pierced. In cases like this the environment from the crucible is basically similar to inside the furnace but substances are prevented from creeping out.